trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Base Information

Chemical Name:trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester
CAS No.:881653-86-7
Molecular Formula:C₂₅H₂₈F₃NO₄S
Molecular Weight:495.563
Hs Code.:

trifluoro-methanesulfonic acid 2-[benzyl-(4-<i>tert</i>-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Synonyms:trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Suppliers and Price of trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

There total 4 articles about trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 881653-84-5
4-tert-butyl-cyclohex-1-enecarboxylic acid benzyl-[2-(tert-butyl-dimethyl-silanyloxy)-phenyl]-amide

: 37595-74-7
N,N-phenylbistrifluoromethane-sulfonimide

: 881653-86-7
trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Guidance literature:: With caesium carbonate; cesium fluoride; In N,N-dimethyl-formamide; at 20 ℃; for 2h;
DOI:10.1021/jo052335a

Reference yield:

: 881653-57-2
N-benzyl-2-((tert-butyldimethylsilyl)oxy)aniline

: 881653-86-7
trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / Bu₃N / Pd(PPh₃)2Cl₂ / dimethylformamide / 2 h / 100 °C

2: 84 percent / cesium fluoride; cesium carbonate / dimethylformamide / 2 h / 20 °C

With tributyl-amine; caesium carbonate; cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; In N,N-dimethyl-formamide;
DOI:10.1021/jo052335a

Reference yield:

: 1624-53-9,3230-45-3,137838-23-4
2-(benzylideneamino)phenol

: 881653-86-7
trifluoro-methanesulfonic acid 2-[benzyl-(4-tert-butyl-cyclohex-1-enecarbonyl)-amino]-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: sodium borohydride / methanol / 0 °C

2: imidazole / CH₂Cl₂

3: 78 percent / Bu₃N / Pd(PPh₃)2Cl₂ / dimethylformamide / 2 h / 100 °C

4: 84 percent / cesium fluoride; cesium carbonate / dimethylformamide / 2 h / 20 °C

With 1H-imidazole; sodium tetrahydroborate; tributyl-amine; caesium carbonate; cesium fluoride; bis-triphenylphosphine-palladium(II) chloride; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jo052335a