(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

Base Information

Chemical Name:(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide
CAS No.:113934-94-4
Molecular Formula:C₂₄H₂₃NO₂S
Molecular Weight:389.518
Hs Code.:

Synonyms:(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

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Chemical Property of (E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

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Technology Process of (E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

There total 4 articles about (E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 66.0%

: 538-56-7
cinnamic acid anhydride

: 113934-91-1
2-(p-methoxyphenyl)-2-(phenylthio)-1-aminoethane

: 113934-94-4
(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; at 25 ℃;
DOI:10.1039/c39870001219

Reference yield:

: 52809-71-9
(1-(4-methoxyphenyl)-2-nitroethyl) phenyl sulfide

: 113934-94-4
(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

Guidance literature:: Multi-step reaction with 2 steps

1: Zn, HCl, AcOH / 2 h / Heating

2: 66 percent / NaHCO₃ / CH₂Cl₂ / 25 °C

With hydrogenchloride; sodium hydrogencarbonate; acetic acid; zinc; In dichloromethane;
DOI:10.1039/c39870001219

Reference yield:

: 123-11-5
4-methoxy-benzaldehyde

: 113934-94-4
(E)-N-[2-(4-Methoxy-phenyl)-2-phenylsulfanyl-ethyl]-3-phenyl-acrylamide

Guidance literature:: Multi-step reaction with 3 steps

1: 86 percent / MeNH₃Cl, Na₂CO₃ / 72 h / 25 °C

2: Zn, HCl, AcOH / 2 h / Heating

3: 66 percent / NaHCO₃ / CH₂Cl₂ / 25 °C

With hydrogenchloride; methylamine hydrochloride; sodium hydrogencarbonate; sodium carbonate; acetic acid; zinc; In dichloromethane;
DOI:10.1039/c39870001219