5-cyclohexylidenepentanoic acid methyl ester

Base Information

Chemical Name:5-cyclohexylidenepentanoic acid methyl ester
CAS No.:503868-31-3
Molecular Formula:C₁₂H₂₀O₂
Molecular Weight:196.29
Hs Code.:

Synonyms:5-cyclohexylidenepentanoic acid methyl ester

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Chemical Property of 5-cyclohexylidenepentanoic acid methyl ester

Chemical Property:

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Technology Process of 5-cyclohexylidenepentanoic acid methyl ester

There total 3 articles about 5-cyclohexylidenepentanoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 67-56-1
methanol

: 26433-79-4
5-cyclohexylidenepentanoic acid

: 503868-31-3
5-cyclohexylidenepentanoic acid methyl ester

Guidance literature:: With sulfuric acid; at 40 ℃; for 3h;
DOI:10.1021/jm020972c

Reference yield:

: 17814-85-6
(4-carboxybutyl)triphenylphosphonium bromide

: 503868-31-3
5-cyclohexylidenepentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: [(CH₃)3Si]2NK / tetrahydrofuran / 0.25 h / 20 °C

1.2: 80 percent / tetrahydrofuran / 3 h / 20 °C

2.1: 93 percent / conc. H₂SO₄ / 3 h / 40 °C

With sulfuric acid; potassium hexamethylsilazane; In tetrahydrofuran; 1.2: Wittig reaction;
DOI:10.1021/jm020972c

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 503868-31-3
5-cyclohexylidenepentanoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1.1: [(CH₃)3Si]2NK / tetrahydrofuran / 0.25 h / 20 °C

1.2: 80 percent / tetrahydrofuran / 3 h / 20 °C

2.1: 93 percent / conc. H₂SO₄ / 3 h / 40 °C

With sulfuric acid; potassium hexamethylsilazane; In tetrahydrofuran; 1.2: Wittig reaction;
DOI:10.1021/jm020972c