S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate

Base Information

• Chemical Name: S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate
• CAS No.: 676557-84-9
• Molecular Formula: C₃₇H₃₄N₆O₃S₃
• Molecular Weight: 706.913

Synonyms:S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate

Chemical Property of S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate

Chemical Property:

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Technology Process of S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate

There total 3 articles about S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

3,3',3-[methylidynetris(1H-pyrazole-1,3-diyl)]tribenzene-methanol (1201681-77-7) + tiolacetic acid (507-09-5) → S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate (676557-84-9)

Guidance literature:

With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 0 - 20 ℃;

DOI:10.1055/s-0029-1216968

Reference yield: 7.0%

tris(3,5-dimethylpyrazolyl)methane (28791-97-1) + ethanethioic acid S-[[3-(1H-pyrazol-3-yl)phenyl]methyl] ester (676557-81-6) → S-[3-(1-acetyl-1H-pyrazol-3-yl)benzyl] ethanethioate (676557-83-8) + S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate (676557-84-9)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; for 48h; Reflux;

DOI:10.1055/s-0029-1216968

Reference yield:

tris(3,5-dimethylpyrazolyl)methane (28791-97-1) + ethanethioic acid S-[[3-(1H-pyrazol-3-yl)phenyl]methyl] ester (676557-81-6) → C30H30N6O2S2 + S,S',S-[methylidynetris(1H-pyrazole-1,3-diyl-3,1-phenylene-methylene)] triethanethioate (676557-84-9)

Guidance literature:

With toluene-4-sulfonic acid; In toluene; Reflux;

DOI:10.1055/s-0029-1216968

upstream raw materials:

3,3',3-[methylidynetris(1H-pyrazole-1,3-diyl)]tribenzene-methanol

tiolacetic acid

tris(3,5-dimethylpyrazolyl)methane

ethanethioic acid S-[[3-(1H-pyrazol-3-yl)phenyl]methyl] ester

Downstream raw materials:

3,3',3-[methylidynetris(1H-pyrazole-1,3-diyl)]tribenzene-methane thiol

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