2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Base Information

Chemical Name:2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane
CAS No.:1369957-04-9
Molecular Formula:C₂₀H₂₄ClN₅
Molecular Weight:369.897
Hs Code.:

Synonyms:2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

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Chemical Property of 2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

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Technology Process of 2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

There total 3 articles about 2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.0%

: 1369956-98-8
1-(2-chlorophenyl)methyl-2-[(4-phenyl-1,2,3-triazol-1-yl)methyl]aziridine

: 506-59-2
N,N-dimethylammonium chloride

: 1369957-04-9
2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Guidance literature:: With dimethyl amine; In acetonitrile; at 140 ℃; for 2h; regioselective reaction; Microwave irradiation;
DOI:10.3762/bjoc.7.205

Reference yield:

: 832724-77-3
2-(bromomethyl)-1-[(2-chlorophenyl)methyl]aziridine

: 1369957-04-9
2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / dimethyl sulfoxide / 16 h / 20 - 80 °C

2: copper(l) iodide / acetonitrile / 16 h / 20 °C / Reflux

3: dimethyl amine / acetonitrile / 2 h / 140 °C / Microwave irradiation

With copper(l) iodide; sodium azide; dimethyl amine; In dimethyl sulfoxide; acetonitrile;
DOI:10.3762/bjoc.7.205

Reference yield:

: 1369956-91-1
2-azidomethyl-1-[(2-chlorophenyl)methyl]aziridine

: 536-74-3
phenylacetylene

: 1369957-04-9
2-[(2-chlorophenyl)methyl]amino-3-dimethylamino-1-(4-phenyl-1,2,3-triazol-1-yl)propane

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide / acetonitrile / 16 h / 20 °C / Reflux

2: dimethyl amine / acetonitrile / 2 h / 140 °C / Microwave irradiation

With copper(l) iodide; dimethyl amine; In acetonitrile;
DOI:10.3762/bjoc.7.205