benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

Base Information

Chemical Name:benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside
CAS No.:55287-53-1
Molecular Formula:C₄₈H₄₇NO₆
Molecular Weight:733.904
Hs Code.:

Synonyms:benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

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Chemical Property of benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

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Technology Process of benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

There total 5 articles about benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 33493-71-9
benzyl 2-acetamido-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

: 100-39-0
benzyl bromide

: 55287-53-1
benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

Guidance literature:: With barium dihydroxide; barium(II) oxide; In N,N-dimethyl-formamide; Ambient temperature; overnight;
DOI:10.1016/0008-6215(88)80153-8

Reference yield:

: 13343-62-9,347411-88-5
benzyl 2-acetamido-2-deoxy-α-D-glucopyranoside

: 55287-53-1
benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine / 5 h / 100 °C

2: 80 percent / NaH / tetrahydrofuran / 0.67 h / Heating

With sodium hydride; In tetrahydrofuran; pyridine; 1: Tritylation / 2: Benzylation;
DOI:10.1002/1099-0690(200009)2000:17<3075::AID-EJOC3075>3.0.CO;2-C

Reference yield:

: 76-83-5
trityl chloride

: 55287-53-1
benzyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-6-O-trityl-α-D-gluco-pyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / pyridine / 5 h / 100 °C

2: 80 percent / NaH / tetrahydrofuran / 0.67 h / Heating

With sodium hydride; In tetrahydrofuran; pyridine; 1: Tritylation / 2: Benzylation;
DOI:10.1002/1099-0690(200009)2000:17<3075::AID-EJOC3075>3.0.CO;2-C