4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Base Information

Chemical Name:4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside
CAS No.:1259298-27-5
Molecular Formula:C₅₀H₅₄O₇Si
Molecular Weight:795.06
Hs Code.:

Synonyms:4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

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Chemical Property of 4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

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Technology Process of 4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

There total 6 articles about 4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 58479-61-1
tert-butylchlorodiphenylsilane

: 1055325-21-7
p-methoxyphenyl 2,3,4-tri-O-benzyl-β-D-glucopyranoside

: 1259298-27-5
4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: With 1H-imidazole; In dichloromethane; for 1h;
DOI:10.1002/chem.201001204

Reference yield: 70.0%

: 1075709-09-9
1-O-p-methoxyphenyl 6-O-tert-butyldiphenylsilyl-β-D-glucopyranose

: 100-39-0
benzyl bromide

: 1259298-27-5
4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 2h;
DOI:10.1039/c3ob40552d

Reference yield:

: 604-69-3
β-D-glucose pentaacetate

: 1259298-27-5
4-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-tert-butyldiphenylsilyl-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine; boron trifluoride diethyl etherate / dichloromethane / 10.5 h / 0 - 20 °C / Inert atmosphere

2.1: sodium methylate / methanol / 1 h / 20 °C

2.2: Amberlite IR-120 resin (H form)

3.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C

4.1: sodium hydride / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With 1H-imidazole; boron trifluoride diethyl etherate; sodium methylate; sodium hydride; triethylamine; In methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c3ob40552d