N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

Base Information

Chemical Name:N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine
CAS No.:735271-42-8
Molecular Formula:C₂₅H₂₅NO₃
Molecular Weight:387.478
Hs Code.:

Synonyms:N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

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Technology Process of N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

There total 3 articles about N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 119-61-9
benzophenone

: 735271-41-7
N-(3-methoxybenzyl)-N-(2-propynyl)-O-methylhydroxylamine

: 735271-42-8
N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

Guidance literature:: With n-butyllithium; In tetrahydrofuran; at 0 ℃; for 0.5h;
DOI:10.1021/ol049301u

Reference yield:

: 874-98-6
1-bromomethyl-3-methoxybenzene

: 735271-42-8
N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 58 percent / iPr₂NEt / dimethylformamide / 19 h / 20 °C

2: 98 percent / iPr₂NEt / dimethylformamide / 15 h / 60 °C

3: 75 percent / BuLi / tetrahydrofuran / 0.5 h / 0 °C

With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol049301u

Reference yield:

: 164934-48-9
N-(3-methoxybenzyl)-O-methylhydroxylamine

: 735271-42-8
N-(3-methoxybenzyl)-N-(4-hydroxy-4,4-diphenyl-2-butynyl)-O-methylhydroxylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / iPr₂NEt / dimethylformamide / 15 h / 60 °C

2: 75 percent / BuLi / tetrahydrofuran / 0.5 h / 0 °C

With n-butyllithium; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/ol049301u