3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

Base Information

Chemical Name:3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide
CAS No.:1198620-80-2
Molecular Formula:C₂₃H₂₂FN₃O₅
Molecular Weight:439.443
Hs Code.:

Synonyms:3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

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Chemical Property of 3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

Chemical Property:

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Technology Process of 3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

There total 3 articles about 3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 1198621-52-1
C₃₉H₄₀FN₃O₅Si

: 1198620-80-2
3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

Reference yield:

: 1198621-50-9
C₃₂H₃₅FN₂O₄Si

: 1198620-80-2
3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

Guidance literature:: Multi-step reaction with 4 steps

1.1: manganese(IV) oxide / chloroform / 20 °C / Reflux

2.1: sodium cyanide / 1 h / 20 °C

3.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

3.2: 0.5 h / -78 °C

4.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

With sodium cyanide; manganese(IV) oxide; tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran; chloroform;

Reference yield:

: 1198621-51-0
C₃₃H₃₅FN₂O₅Si

: 2687-43-6
O-benzylhydoxylamine hydrochloride

: 1198620-80-2
3-hydroxy-4-hydroxymethyl-pyridine-2,5-dicarboxylic acid 5-cyclohexylmethyl-amide 2-hydroxyamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: lithium hexamethyldisilazane / tetrahydrofuran / -78 °C

1.2: 0.5 h / -78 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C

With tetrabutyl ammonium fluoride; lithium hexamethyldisilazane; In tetrahydrofuran;