C₂₈H₄₄O₃

Base Information

Chemical Name:C₂₈H₄₄O₃
CAS No.:1409941-45-2
Molecular Formula:C₂₈H₄₄O₃
Molecular Weight:428.656
Hs Code.:

C<sub>28</sub>H<sub>44</sub>O<sub>3</sub>

Synonyms:C₂₈H₄₄O₃

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Chemical Property of C₂₈H₄₄O₃

Chemical Property:

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Technology Process of C₂₈H₄₄O₃

There total 5 articles about C₂₈H₄₄O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 1409941-44-1
C₁₅H₁₈O₄

: 13266-02-9
n-tridecyltriphenylphosphonium bromide

: 1409941-45-2
C₂₈H₄₄O₃

Guidance literature:: n-tridecyltriphenylphosphonium bromide; With sodium hexamethyldisilazane; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

C₁₅H₁₈O₄; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol302820c

Reference yield:

: 100-39-0
benzyl bromide

: 1409941-45-2
C₂₈H₄₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: peracetic acid; acetic acid / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dimethylsulfide borane complex / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

3.1: dimethyl sulfoxide; oxalyl dichloride; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

With peracetic acid; oxalyl dichloride; dimethylsulfide borane complex; sodium hexamethyldisilazane; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 3.1: |Swern Oxidation / 4.1: |Wittig Olefination;
DOI:10.1021/ol302820c

Reference yield:

: 1552-12-1,111-78-4
1,5-cis,cis-cyclooctadiene

: 1409941-45-2
C₂₈H₄₄O₃

Guidance literature:: Multi-step reaction with 4 steps

1.1: peracetic acid; acetic acid / 0 - 20 °C / Inert atmosphere

1.2: 20 °C / Inert atmosphere

2.1: dimethylsulfide borane complex / tetrahydrofuran / -15 - 20 °C / Inert atmosphere

3.1: dimethyl sulfoxide; oxalyl dichloride; triethylamine / dichloromethane / -78 - 20 °C / Inert atmosphere

4.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

4.2: -78 - 20 °C / Inert atmosphere

With peracetic acid; oxalyl dichloride; dimethylsulfide borane complex; sodium hexamethyldisilazane; acetic acid; dimethyl sulfoxide; triethylamine; In tetrahydrofuran; dichloromethane; 3.1: |Swern Oxidation / 4.1: |Wittig Olefination;
DOI:10.1021/ol302820c