(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

Base Information

Chemical Name:(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide
CAS No.:1144108-49-5
Molecular Formula:C₁₃H₁₅F₆NOS
Molecular Weight:347.325
Hs Code.:

Synonyms:(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

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Technology Process of (S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

There total 4 articles about (S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 48.0%

: 1144108-49-5
(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: In toluene; at -78 ℃; for 0.25h; Glovebox; Inert atmosphere;

With potassium hexamethylsilazane; In toluene; at -78 ℃;

Reference yield:

: 75-46-7
trifluoromethan

: 607729-60-2
(S)-2-methyl-N-[[4-(trifluoromethyl)phenyl]methylidene]propane-2-sulfinamide

: 1144108-49-5
(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

: (S)-2-methyl-N-((R)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: With potassium hexamethylsilazane; In toluene; at -78 ℃; Overall yield = 42 %; Overall yield = 48 %Spectr.; diastereoselective reaction; Inert atmosphere; Glovebox;
DOI:10.1039/c8cc01526k

Reference yield:

: 1219607-83-6
(S_S)-2-methyl-N-(2,2,2-trifluoroethylidene)-propane-2-sulfinamide

: 128796-39-4
4-trifluoromethylphenylboronic acid

: 1144108-49-5
(S)-2-methyl-N-((S)-2,2,2-trifluoro-1-(4-(trifluoromethyl)phenyl)ethyl)propane-2-sulfinamide

Guidance literature:: With [Rh(OH)(cod)]2; triethylamine; In dichloromethane; at 0 ℃; for 18h; optical yield given as %de; diastereoselective reaction; Inert atmosphere;
DOI:10.1016/j.tetlet.2009.01.112