(2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate

Base Information

• Chemical Name: (2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate
• CAS No.: 137719-75-6
• Molecular Formula: C₁₈H₂₇NO₄S
• Molecular Weight: 353.483
• Mol file: 137719-75-6.mol

Synonyms:(2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate

Chemical Property of (2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of (2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate

There total 1 articles about (2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

tert-butyl [(2R,3R)-3-(benzyloxy)-1-hydroxybutan-2-yl]carbamate (79069-63-9,133565-43-2) + tiolacetic acid (507-09-5) → (2S,3R)-3-(benzyloxy)-2-<(tert-butoxycarbonyl)amino>butyl ethanethioate (137719-75-6)

Guidance literature:

With triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; 2 h at 0 deg C and 20 h at r.t.;

DOI:10.1021/jo00028a071

upstream raw materials:

tert-butyl [(2R,3R)-3-(benzyloxy)-1-hydroxybutan-2-yl]carbamate

tiolacetic acid