N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

Base Information

Chemical Name:N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide
CAS No.:868961-36-8
Molecular Formula:C₁₉H₂₅IN₂
Molecular Weight:408.325
Hs Code.:

Synonyms:N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

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Chemical Property of N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

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Technology Process of N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

There total 5 articles about N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 868961-60-8
N-(4-bromo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

: 868961-36-8
N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

Guidance literature:: With copper(l) iodide; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; at 115 - 120 ℃; for 24h;
DOI:10.1021/ol0516521

Reference yield:

: 868961-34-6
oxo-(2,4,6-trimethylphenylamino)acetyl chloride

: 868961-36-8
N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

Guidance literature:: Multi-step reaction with 3 steps

1.1: 73 percent / Et₃N / CH₂Cl₂ / 15 h / 20 °C

2.1: BH₃*Me₂S / toluene / 18 h / 95 °C

2.2: aq. HCl / toluene / pH 3

2.3: 58 percent / Et₃N / CH₂Cl₂ / 7 h / 20 °C

3.1: 94 percent / CuI; NaI; N,N'-dimethylethylenediamine / dioxane / 24 h / 115 - 120 °C

With copper(l) iodide; dimethylsulfide borane complex; triethylamine; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; dichloromethane; toluene;
DOI:10.1021/ol0516521

Reference yield:

: 868961-35-7
N-(4-bromo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)oxamide

: 868961-36-8
N-(4-iodo-2,6-dimethylphenyl)-N'-(2,4,6-trimethylphenyl)ethane-1,2-diamineoxamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: BH₃*Me₂S / toluene / 18 h / 95 °C

1.2: aq. HCl / toluene / pH 3

1.3: 58 percent / Et₃N / CH₂Cl₂ / 7 h / 20 °C

2.1: 94 percent / CuI; NaI; N,N'-dimethylethylenediamine / dioxane / 24 h / 115 - 120 °C

With copper(l) iodide; dimethylsulfide borane complex; sodium iodide; N,N`-dimethylethylenediamine; In 1,4-dioxane; toluene;
DOI:10.1021/ol0516521