allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Base Information

Chemical Name:allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside
CAS No.:1603827-00-4
Molecular Formula:C₅₇H₆₀Cl₃NO₁₄
Molecular Weight:1089.46
Hs Code.:

allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Synonyms:allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Chemical Property of allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

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Technology Process of allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

There total 3 articles about allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1603826-97-6
allyl (benzyl 2,3-di-O-benzyl-β-D-gatactopyranosyturonate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 123-76-2
levulinic acid

: 1603827-00-4
allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; for 16h; Inert atmosphere;

Reference yield:

: 1603826-98-7
allyl (2,3-di-O-benzyl-β-D-galactopyranosyl)-(1-3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

: 1603827-00-4
allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 20 °C

1.2: 16 h / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 16 h / Inert atmosphere

With dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; dicyclohexyl-carbodiimide; In dichloromethane; water;

Reference yield:

: 100-39-0
benzyl bromide

: 1603827-00-4
allyl (benzyl 2,3-di-O-benzyl-4-O-levulinoyl-β-D-galactopyranosyluronate)-(1→3)-4,6-di-O-benzyl-2-deoxy-2-trichloroacetamido-β-D-galactopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1.1: 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical / dichloromethane; water / 1.5 h / 20 °C

1.2: 16 h / Inert atmosphere

2.1: dicyclohexyl-carbodiimide; dmap / dichloromethane / 16 h / Inert atmosphere

With dmap; 2,2,6,6-Tetramethyl-1-piperidinyloxy free radical; dicyclohexyl-carbodiimide; In dichloromethane; water;