C₂₆H₃₄FN₃O₄Si

Base Information

Chemical Name:C₂₆H₃₄FN₃O₄Si
CAS No.:1374110-09-4
Molecular Formula:C₂₆H₃₄FN₃O₄Si
Molecular Weight:499.658
Hs Code.:

C<sub>26</sub>H<sub>34</sub>FN<sub>3</sub>O<sub>4</sub>Si

Synonyms:C₂₆H₃₄FN₃O₄Si

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Chemical Property of C₂₆H₃₄FN₃O₄Si

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Technology Process of C₂₆H₃₄FN₃O₄Si

There total 4 articles about C₂₆H₃₄FN₃O₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 1374108-27-6
2-tert-butyldimethylsiloxy-3-fluoro-1-propanol

: 1374110-04-9
C₁₇H₁₅N₃O₃

: 1374110-09-4
C₂₆H₃₄FN₃O₄Si

Guidance literature:: With di-isopropyl azodicarboxylate; triphenylphosphine; In tetrahydrofuran; at 20 ℃; for 17h; Cooling with ice;

Reference yield:

: 755026-96-1
2-(3-methoxy-4-nitrophenyl)-4,4,5,5-tetramethyl-[1,3,2]dioxaborolane

: 1374110-09-4
C₂₆H₃₄FN₃O₄Si

Guidance literature:: Multi-step reaction with 3 steps

1: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

2: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere

3: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 20 °C / Cooling with ice

With N,N,N,N,N,N-hexamethylphosphoric triamide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; potassium carbonate; triphenylphosphine; lithium chloride; In tetrahydrofuran; 1,2-dimethoxyethane; water;

Reference yield:

: 6627-53-8
1-chloro-3-methoxy-4-nitrobenzene

: 1374110-09-4
C₂₆H₃₄FN₃O₄Si

Guidance literature:: Multi-step reaction with 4 steps

1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; potassium acetate; tricyclohexylphosphine / 1,4-dioxane / 16 h / 90 °C / Inert atmosphere

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / water; 1,2-dimethoxyethane / 16 h / 80 °C / Inert atmosphere

3: lithium chloride; N,N,N,N,N,N-hexamethylphosphoric triamide / 16 h / 110 °C / Inert atmosphere

4: triphenylphosphine; di-isopropyl azodicarboxylate / tetrahydrofuran / 17 h / 20 °C / Cooling with ice

With N,N,N,N,N,N-hexamethylphosphoric triamide; tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; tetrakis(triphenylphosphine) palladium⁽⁰⁾; di-isopropyl azodicarboxylate; potassium acetate; potassium carbonate; triphenylphosphine; lithium chloride; tricyclohexylphosphine; In tetrahydrofuran; 1,4-dioxane; 1,2-dimethoxyethane; water;