C₂₇H₂₄N₂O₇S

Base Information

Chemical Name:C₂₇H₂₄N₂O₇S
CAS No.:1380111-46-5
Molecular Formula:C₂₇H₂₄N₂O₇S
Molecular Weight:520.563
Hs Code.:

C<sub>27</sub>H<sub>24</sub>N<sub>2</sub>O<sub>7</sub>S

Synonyms:C₂₇H₂₄N₂O₇S

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Chemical Property of C₂₇H₂₄N₂O₇S

Chemical Property:

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Technology Process of C₂₇H₂₄N₂O₇S

There total 8 articles about C₂₇H₂₄N₂O₇S which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.1%

: 10130-89-9
p-carboxyphenylsulfonyl chloride

: 1380112-29-7
CH₄O₃S*C₂₀H₂₀N₂O₃

: 1380111-46-5
C₂₇H₂₄N₂O₇S

Guidance literature:: CH₄O₃S*C₂₀H₂₀N₂O₃; With potassium phosphate; In dichloromethane; water; for 0.5h;

p-carboxyphenylsulfonyl chloride; With sodium hydrogencarbonate; In water; acetonitrile; at 20 - 25 ℃; for 10h;

Reference yield:

: 100-39-0
benzyl bromide

: 1380111-46-5
C₂₇H₂₄N₂O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: water; ethyl acetate / 20 - 50 °C

8.1: potassium phosphate / dichloromethane; water / 0.5 h

8.2: 10 h / 20 - 25 °C

With potassium phosphate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;

Reference yield:

: 501-30-4,123712-78-7
5-hydroxy-2-(hydroxymethyl)-4H-pyran-4-one

: 1380111-46-5
C₂₇H₂₄N₂O₇S

Guidance literature:: Multi-step reaction with 8 steps

1.1: sodium hydroxide / methanol; water / Reflux

2.1: hydroxylamine hydrochloride; sodium acetate / ethanol; water / 60 °C

3.1: potassium carbonate / dimethyl sulfoxide / 1 h / 20 - 25 °C

4.1: triethylamine / dichloromethane / 1 h / 0 °C

5.1: potassium iodide / N,N-dimethyl-formamide / 20 - 25 °C

6.1: hydrazine hydrate / ethanol / 1 h / Reflux

7.1: water; ethyl acetate / 20 - 50 °C

8.1: potassium phosphate / dichloromethane; water / 0.5 h

8.2: 10 h / 20 - 25 °C

With potassium phosphate; hydroxylamine hydrochloride; sodium acetate; potassium carbonate; hydrazine hydrate; triethylamine; potassium iodide; sodium hydroxide; In methanol; ethanol; dichloromethane; water; dimethyl sulfoxide; ethyl acetate; N,N-dimethyl-formamide;