1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane
CAS No.:1331909-82-0
Molecular Formula:C₃₀H₅₃N₅O₄
Molecular Weight:547.782
Hs Code.:

Synonyms:1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

There total 5 articles about 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1331909-77-3
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

: 1331909-82-0
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With hydrogen; lead; Pd*CaCO₃; In ethanol; at 20 ℃; for 12h;

Reference yield:

: 852921-64-3
1,8-N,N′-bis(carbo-tert-butoxymethyl)-1,4,8,11-tetraazacyclotetradecane

: 1331909-82-0
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate; potassium iodide / toluene / 24 h / Reflux

2: hydrogen / lead; Pd*CaCO₃ / ethanol / 12 h / 20 °C

With hydrogen; potassium carbonate; potassium iodide; lead; Pd*CaCO₃; In ethanol; toluene;

Reference yield:

: 75920-10-4
1,4,8,11-tetraazatricyclo[9.3.1.14,8]hexadecane

: 1331909-82-0
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-aminophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 4 steps

1: acetonitrile / 24 h / 20 °C

2: sodium hydroxide / 3 h

3: potassium carbonate; potassium iodide / toluene / 24 h / Reflux

4: hydrogen / lead; Pd*CaCO₃ / ethanol / 12 h / 20 °C

With hydrogen; potassium carbonate; potassium iodide; sodium hydroxide; lead; Pd*CaCO₃; In ethanol; toluene; acetonitrile;