1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

Base Information

Chemical Name:1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane
CAS No.:1331909-77-3
Molecular Formula:C₃₀H₅₁N₅O₆
Molecular Weight:577.765
Hs Code.:

Synonyms:1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

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Chemical Property of 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

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Technology Process of 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

There total 4 articles about 1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 5339-26-4
(4-nitrophenyl)ethyl bromide

: 852921-64-3
1,8-N,N′-bis(carbo-tert-butoxymethyl)-1,4,8,11-tetraazacyclotetradecane

: 1331909-77-3
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: With potassium carbonate; potassium iodide; In toluene; for 24h; Reflux;

Reference yield:

: 5292-43-3
bromoacetic acid tert-butyl ester

: 1331909-77-3
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 24 h / 20 °C

2: sodium hydroxide / 3 h

3: potassium carbonate; potassium iodide / toluene / 24 h / Reflux

With potassium carbonate; potassium iodide; sodium hydroxide; In toluene; acetonitrile;

Reference yield:

: 75920-10-4
1,4,8,11-tetraazatricyclo[9.3.1.14,8]hexadecane

: 1331909-77-3
1,8-bis-(carbo-tert-butoxymethyl)-4-(4'-nitrophenethyl)-1,4,8,11-tetraazacyclotetradecane

Guidance literature:: Multi-step reaction with 3 steps

1: acetonitrile / 24 h / 20 °C

2: sodium hydroxide / 3 h

3: potassium carbonate; potassium iodide / toluene / 24 h / Reflux

With potassium carbonate; potassium iodide; sodium hydroxide; In toluene; acetonitrile;