2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

Base Information

Chemical Name:2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene
CAS No.:112503-50-1
Molecular Formula:C₂₂H₃₇ClO₂
Molecular Weight:368.988
Hs Code.:

Synonyms:2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

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Chemical Property of 2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

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Technology Process of 2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

There total 8 articles about 2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid (2Z,6E)-3-dimethoxymethyl-7-methyl-9-(2,6,6-trimethyl-cyclohex-1-enyl)-nona-2,6-dienyl ester

: 112503-50-1
2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:: With lithium chloride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h; Yield given;
DOI:10.1016/S0040-4039(00)98937-8

Reference yield:

: 4179-00-4
Methyl (E)-3-methyl-5-(2,6,6-trimethylcyclohexen-1-yl)-2-pentenoate

: 112503-50-1
2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:: Multi-step reaction with 8 steps

1: lithium aluminium hydride

2: PBr₃ / pyridine

4: 2N HCl / 0.05 h / 0 °C

6: 95 percent / diisobutylaluminium hydride / CH₂Cl₂

7: DMAP, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

8: LiCl / dimethylformamide / 0.5 h / 0 °C

With hydrogenchloride; dmap; lithium aluminium tetrahydride; phosphorus tribromide; diisobutylaluminium hydride; triethylamine; lithium chloride; In pyridine; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)98937-8

Reference yield:

: 29550-53-6
(E)-3-methyl-5-(2',6',6'-trimethylcyclohex-1'-enyl)pent-2-enyl bromide

: 112503-50-1
2-((3E,7Z)-9-Chloro-7-dimethoxymethyl-3-methyl-nona-3,7-dienyl)-1,3,3-trimethyl-cyclohexene

Guidance literature:: Multi-step reaction with 6 steps

2: 2N HCl / 0.05 h / 0 °C

4: 95 percent / diisobutylaluminium hydride / CH₂Cl₂

5: DMAP, Et₃N / CH₂Cl₂ / 0.5 h / 0 °C

6: LiCl / dimethylformamide / 0.5 h / 0 °C

With hydrogenchloride; dmap; diisobutylaluminium hydride; triethylamine; lithium chloride; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)98937-8