2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide

Base Information

• Chemical Name: 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide
• CAS No.: 58917-66-1
• Molecular Formula: C₁₇H₁₇N₅O₆
• Molecular Weight: 387.352

Synonyms:2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide

Chemical Property of 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide

There total 4 articles about 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

AICA riboside (2627-69-2) → 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide (58917-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide / 4 h / Ambient temperature

2: aq. sodium hydroxide, iodomethane

With sodium hydroxide; methyl iodide; In N,N-dimethyl-formamide;

Reference yield:

Benzoyl isothiocyanate (532-55-8) → 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide (58917-66-1)

Guidance literature:

Multi-step reaction with 2 steps

1: dimethylformamide / 4 h / Ambient temperature

2: aq. sodium hydroxide, iodomethane

With sodium hydroxide; methyl iodide; In N,N-dimethyl-formamide;

Reference yield:

5-(3-Benzoyl-thioureido)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxylic acid amide (112156-61-3) → 2',1''-anhydro-5-<(1''-benzamido-1''-hydroxymethylene)amino>-1-(β-D-ribofuranosyl)imidazole-4-carboxamide (58917-66-1)

Guidance literature:

With sodium hydroxide; methyl iodide;

DOI:10.1039/c39860000901

upstream raw materials:

5-(3-Benzoyl-thioureido)-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-1H-imidazole-4-carboxylic acid amide

AICA riboside

Benzoyl isothiocyanate

Downstream raw materials:

N₂-Methylguanosine

1-methylguanosine

G

<15NH2>guanosine

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