S-ethyl O-benzyl carbonothioate

Base Information

Chemical Name:S-ethyl O-benzyl carbonothioate
CAS No.:110177-67-8
Molecular Formula:C₁₀H₁₂O₂S
Molecular Weight:196.27
Hs Code.:

Synonyms:S-ethyl O-benzyl carbonothioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of S-ethyl O-benzyl carbonothioate

Chemical Property:

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Technology Process of S-ethyl O-benzyl carbonothioate

There total 3 articles about S-ethyl O-benzyl carbonothioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 463-58-1
carbon oxide sulfide

: 75-03-6
ethyl iodide

: 100-51-6,185532-71-2
benzyl alcohol

: 110177-67-8
S-ethyl O-benzyl carbonothioate

Guidance literature:: carbon oxide sulfide; benzyl alcohol; With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran; at 20 ℃; for 1h; under 750.06 Torr;

ethyl iodide; In tetrahydrofuran; at 20 ℃; for 2h; under 750.06 Torr;
DOI:10.1016/S0040-4020(02)01331-5

Reference yield:

: 125178-42-9
Thiocarbonic acid O-benzyl ester

: 75-03-6
ethyl iodide

: 110177-67-8
S-ethyl O-benzyl carbonothioate

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 2h; under 750.06 Torr;
DOI:10.1016/S0040-4039(02)01834-8

Reference yield:

: 100-51-6,185532-71-2
benzyl alcohol

: 110177-67-8
S-ethyl O-benzyl carbonothioate

Guidance literature:: Multi-step reaction with 2 steps

1: DBU / tetrahydrofuran / 1 h / 20 °C / 750.06 Torr

2: tetrahydrofuran / 2 h / 20 °C / 750.06 Torr

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In tetrahydrofuran;
DOI:10.1016/S0040-4039(02)01834-8