(N-allyl,N-ethylamino)phenylvinylborane

Base Information

Chemical Name:(N-allyl,N-ethylamino)phenylvinylborane
CAS No.:386708-29-8
Molecular Formula:C₁₃H₁₈BN
Molecular Weight:199.104
Hs Code.:

Synonyms:(N-allyl,N-ethylamino)phenylvinylborane

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Chemical Property of (N-allyl,N-ethylamino)phenylvinylborane

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Technology Process of (N-allyl,N-ethylamino)phenylvinylborane

There total 2 articles about (N-allyl,N-ethylamino)phenylvinylborane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 2424-02-4
allylethylamine

: 287735-76-6
phenyl vinyl boron chloride

: 386708-29-8
(N-allyl,N-ethylamino)phenylvinylborane

Guidance literature:: With triethylamine; In dichloromethane; under N2; a soln. of N-allyl,N-ethylamine in CH2Cl2 was added to a soln.of phenylvinylboron chloride in CH2Cl2 at -78°C with stirring, t he mixt. was stirred for 1h, trimethylamine was added, the mixt. was warmed to 25°C for 3 h; the solid was removed by filtration, the solvent was removed in vac., the residue was distilled in vac.; elem. anal.;
DOI:10.1021/om0106635

Reference yield:

: 873-51-8
phenylborondichloride

: 386708-29-8
(N-allyl,N-ethylamino)phenylvinylborane

Guidance literature:: DOI:10.1080/10426500490426610

Reference yield: 85.0%

: 386708-29-8
(N-allyl,N-ethylamino)phenylvinylborane

: 615253-81-1
1-ethyl-2,5-dihydro-2-phenyl-1H-1,2-azaborole

Guidance literature:: Grubbs catalyst first generation; In dichloromethane; under N2; a soln. of the azaborole in CH2Cl2 was added to a soln. of thecatalyst in CH2Cl2 at 25°C, the mixt. was stirred at 25°C for 10 h; the solvent was removed in vac.; elem. anal.;
DOI:10.1021/om0106635