1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Base Information

Chemical Name:1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole
CAS No.:615253-90-2
Molecular Formula:C₁₈H₂₄BNSi
Molecular Weight:293.292
Hs Code.:

Synonyms:

Suppliers and Price of 1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

There total 5 articles about 1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 615253-88-8
1-ethyl-3-chlorodimethylsilyl-2,3-dihydro-2-phenyl-1H-1,2-azaborole

: 16733-97-4
cyclopentadienyllithium

: 615253-90-2
1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Guidance literature:: In tetrahydrofuran; under Ar or N2, 1 equiv. of Li-compd. in THF was added to THF soln. of Si-compd. at -50 °C, warming to 25 °C and stirring for 12 h; solvent was removed in vac., residue was extd. with pentane, solvent wasremoved;
DOI:10.1016/j.poly.2005.03.001

Reference yield:

: 287735-76-6
phenyl vinyl boron chloride

: 615253-90-2
1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Guidance literature:: Multi-step reaction with 5 steps

1: Et₃N / dichloromethane

2: Grubbs catalyst first generation / dichloromethane

4: diethyl ether

5: tetrahydrofuran

With Et₃N; Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.poly.2005.03.001

Reference yield:

: 386708-29-8
(N-allyl,N-ethylamino)phenylvinylborane

: 615253-90-2
1-ethyl-3-(cyclopentadienyldimethylsilyl)-2,3-dihydro-2-phenyl-1H-1,2-azaborole

Guidance literature:: Multi-step reaction with 4 steps

1: Grubbs catalyst first generation / dichloromethane

3: diethyl ether

4: tetrahydrofuran

Grubbs catalyst first generation; In tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1016/j.poly.2005.03.001