(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

Base Information

Chemical Name:(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside
CAS No.:250584-41-9
Molecular Formula:C₃₅H₄₄O₉
Molecular Weight:608.729
Hs Code.:

Synonyms:(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

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Chemical Property of (6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

Chemical Property:

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Technology Process of (6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

There total 7 articles about (6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 100-39-0
benzyl bromide

: 250584-40-8
(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-hydroxymethyl-6,7-O-isopropyl-α-D-galacto/α-D-gluco/β-L-altrofuranoside

: 250584-41-9
(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

: 250584-44-2
(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-β-L-altrofuranoside

: (6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-glucofuranoside

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 1.5h;
DOI:10.1016/S0040-4020(99)00637-7

Reference yield:

: 15186-48-8
2,3-isopropylidene-glyceraldehyde

: 250584-41-9
(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / KHMDS; CeCl₃ / toluene; tetrahydrofuran / -100 - -20 °C

2: 68 percent / LiAlH₄ / diethyl ether / 2 h / 20 °C

3: NaH / dimethylformamide / 1.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; cerium(III) chloride; potassium hexamethylsilazane; sodium hydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene; 1: Condensation / 2: Reduction / 3: Alkylation;
DOI:10.1016/S0040-4020(99)00637-7

Reference yield:

: 217324-99-7
methyl (methyl-3-O-benzyl-2-O-methoxymethyl-α-D-xylofuranoside) uronate

: 250584-41-9
(6R)-methyl-3-O-benzyl-2-O-methoxymethyl-4-C-benzyloxymethyl-6,7-O-isopropyl-α-D-galactofuranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / KHMDS; CeCl₃ / toluene; tetrahydrofuran / -100 - -20 °C

2: 68 percent / LiAlH₄ / diethyl ether / 2 h / 20 °C

3: NaH / dimethylformamide / 1.5 h / 0 - 20 °C

With lithium aluminium tetrahydride; cerium(III) chloride; potassium hexamethylsilazane; sodium hydride; In tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide; toluene; 1: Condensation / 2: Reduction / 3: Alkylation;
DOI:10.1016/S0040-4020(99)00637-7