4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

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Chemical Name:4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside
CAS No.:211677-97-3
Molecular Formula:C₃₄H₃₅N₃O₄S
Molecular Weight:581.736
Hs Code.:

Synonyms:4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

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Chemical Property of 4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

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Technology Process of 4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

There total 9 articles about 4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 5-azido-2-benzyloxymethyl-6-p-tolylsulfanyl-tetrahydro-pyran-3,4-diol

: 100-39-0
benzyl bromide

: p-tolyl 2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-galactopyranside

: 3-azido-5-benzyloxy-6-benzyloxymethyl-2-p-tolylsulfanyl-tetrahydro-pyran-4-ol

: 211677-97-3
4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

Guidance literature:: 5-azido-2-benzyloxymethyl-6-p-tolylsulfanyl-tetrahydro-pyran-3,4-diol; With sodium hydride; In N,N-dimethyl-formamide; at -15 ℃; for 0.0833333h;

benzyl bromide; In N,N-dimethyl-formamide; at -15 - 20 ℃; for 0.5h;
DOI:10.1055/s-2006-939681

Reference yield: 43.0%

: 100-39-0
benzyl bromide

: p-tolyl 2-deoxy-2-azido-1-thio-α/β-D-galactopyranoside

: 211677-97-3
4-methylphenyl 2-azido-3,4,6-tri-O-benzyl-2-deoxy-1-thio-β-D-galactopyranosside

: p-methylphenyl 3,4,6-tri-O-benzyl-2-deoxy-2-azido-1-thio-α-D-galactopyranoside

Guidance literature:: p-tolyl 2-deoxy-2-azido-1-thio-α/β-D-galactopyranoside; With sodium hydride; In N,N-dimethyl-formamide; for 0.166667h;

benzyl bromide; In N,N-dimethyl-formamide; at 20 ℃; for 3h; Further stages.;
DOI:10.1021/jo991558w