phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

Base Information

Chemical Name:phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)
CAS No.:1253183-67-3
Molecular Formula:C₅₇H₅₉N₃O₁₁S
Molecular Weight:994.175
Hs Code.:

Synonyms:phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

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Chemical Property of phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

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Technology Process of phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

There total 1 articles about phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1253183-63-9
tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-1-O-trichloroacetimidoyl-α-D-glucopyranosyl)uronate

: 277756-87-3
phenyl 2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside

: 1253183-67-3
phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

Guidance literature:: With trimethylsilyl trifluoromethanesulfonate; In toluene; at -30 ℃; for 1.5h; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.08.004

Reference yield: 56.0%

: 1253183-73-1
methyl [tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

: 1253183-67-3
phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

: 1253183-83-3
methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-[tert-butyl (2-O-benzoyl-3-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In diethyl ether; dichloromethane; at 0 - 20 ℃; for 48h; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.08.004

Reference yield: 40.0%

: 1253183-75-3
methyl (2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

: 1253183-67-3
phenyl [tert-butyl (3,4-di-O-benzyl-2-O-benzoyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-1-thio-β-D-glucopyranoside)

: 1253183-79-7
methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-β-D-glucopyranosyl)-(1->4)-(2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

: 1253183-77-5
methyl [tert-butyl (2-O-benzoyl-3,4-di-O-benzyl-β-D-glucopyranosyl)uronate]-(1->4)-(2-azido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranosyl)-(1->4)-(2-O-benzoyl-3-O-benzyl-6-O-chloroacetyl-β-D-glucopyranosyl)-(1->4)-(2-acetamido-3,6-di-O-benzyl-2-deoxy-α-D-glucopyranoside)

Guidance literature:: With 2,6-di-tert-butyl-4-methylpyridine; dimethyl-(methylthio)-sulphonium trifluoromethanesulphonate; In diethyl ether; dichloromethane; at 0 - 20 ℃; stereoselective reaction; Molecular sieve; Inert atmosphere;
DOI:10.1016/j.tet.2010.08.004