C₂₁H₂₁NO

Base Information

Chemical Name:C₂₁H₂₁NO
CAS No.:1356380-99-8
Molecular Formula:C₂₁H₂₁NO
Molecular Weight:303.404
Hs Code.:

Synonyms:C₂₁H₂₁NO

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Chemical Property of C₂₁H₂₁NO

Chemical Property:

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Technology Process of C₂₁H₂₁NO

There total 8 articles about C₂₁H₂₁NO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1356380-98-7
C₂₄H₂₇NO₂

: 1356380-99-8
C₂₁H₂₁NO

Guidance literature:: C₂₄H₂₇NO₂; With potassium tert-butylate; In tert-butyl alcohol; at 35 - 82 ℃; for 10h; degassed;

With water;

Reference yield:

: 540-38-5
p-Iodophenol

: 1356380-99-8
C₂₁H₂₁NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 20 °C

2.1: diisopropylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / chloroform / 25 h / 20 °C / degassed

3.1: potassium tert-butylate / tert-butyl alcohol / 10 h / 45 - 82.5 °C / degassed

3.2: Cooling with ice

4.1: diisopropylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / chloroform / 5 h / 20 °C / degassed

5.1: potassium tert-butylate / tert-butyl alcohol / 10 h / 35 - 82 °C / degassed

With potassium tert-butylate; diisopropylamine; potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In chloroform; dimethyl sulfoxide; tert-butyl alcohol;

Reference yield:

: 5407-04-5
3-(dimethylamino)propyl chloride hydrochloride

: 1356380-99-8
C₂₁H₂₁NO

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium hydroxide / dimethyl sulfoxide / 20 °C

2.1: diisopropylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / chloroform / 25 h / 20 °C / degassed

3.1: potassium tert-butylate / tert-butyl alcohol / 10 h / 45 - 82.5 °C / degassed

3.2: Cooling with ice

4.1: diisopropylamine / copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride / chloroform / 5 h / 20 °C / degassed

5.1: potassium tert-butylate / tert-butyl alcohol / 10 h / 35 - 82 °C / degassed

With potassium tert-butylate; diisopropylamine; potassium hydroxide; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; In chloroform; dimethyl sulfoxide; tert-butyl alcohol;