3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

Base Information

Chemical Name:3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione
CAS No.:1420039-64-0
Molecular Formula:C₂₉H₄₆O₅Si₂
Molecular Weight:530.852
Hs Code.:

Synonyms:3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

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Chemical Property of 3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

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Technology Process of 3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

There total 13 articles about 3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1420039-62-8
3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-2-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)-2-hydroxysuccinic acid

: 1420039-64-0
3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

Guidance literature:: With acetic anhydride; at 120 ℃; for 18h;

Reference yield:

: 31770-76-0
3-(4-hydroxyphenyl)propionic acid benzyl ester

: 1420039-64-0
3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

Guidance literature:: Multi-step reaction with 4 steps

1.1: 1H-imidazole / dichloromethane / 15 h / 0 - 20 °C

2.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.5 h / -78 - 0 °C / Inert atmosphere

2.2: 1 h / -78 °C

3.1: palladium 10% on activated carbon; hydrogen / 24 h / Inert atmosphere

4.1: acetic anhydride / 18 h / 120 °C

With 1H-imidazole; n-butyllithium; palladium 10% on activated carbon; hydrogen; acetic anhydride; diisopropylamine; In tetrahydrofuran; hexane; dichloromethane;

Reference yield:

: 929556-81-0
benzyl 3-(4-((tert-butyldimethylsilyl)oxy)phenyl)propanoate

: 1420039-64-0
3-(4-((tert-butyldimethylsilyl)oxy)benzyl)-4-(cis-4-((tert-butyldimethylsilyl)oxy)cyclohexyl)furan-2,5-dione

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium; diisopropylamine / tetrahydrofuran; hexane / 1.5 h / -78 - 0 °C / Inert atmosphere

1.2: 1 h / -78 °C

2.1: palladium 10% on activated carbon; hydrogen / 24 h / Inert atmosphere

3.1: acetic anhydride / 18 h / 120 °C

With n-butyllithium; palladium 10% on activated carbon; hydrogen; acetic anhydride; diisopropylamine; In tetrahydrofuran; hexane;