cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

Base Information

Chemical Name:cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine
CAS No.:950772-67-5
Molecular Formula:C₂₂H₃₅N₃O₃
Molecular Weight:389.538
Hs Code.:

Synonyms:cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

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Chemical Property of cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

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Technology Process of cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

There total 3 articles about cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: cis/trans 1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine dihydrochloride

: 446-34-4
2-fluoro-4-methyl-1-nitrobenzene

: 950772-68-6
trans N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

: 950772-67-5
cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 - 100 ℃;

Reference yield:

: 950772-65-3
cis/trans 1,1-dimethylethyl {1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinyl}carbamate

: 950772-67-5
cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / 1,4-dioxane; diethyl ether / 6 h / 20 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 100 °C

With hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide;

Reference yield:

: 73874-95-0
(piperidin-4-yl)carbamic acid tert-butyl ester

: 950772-67-5
cis N-(5-methyl-2-nitrophenyl)-1-[1-methyl-4-(propyloxy)cyclohexyl]-4-piperidinamine

Guidance literature:: Multi-step reaction with 3 steps

1.1: 1,2,3-triazole / toluene / 6 h / 130 °C / Heating / reflux

1.2: 0 - 25 °C

2.1: hydrogenchloride / 1,4-dioxane; diethyl ether / 6 h / 20 °C

3.1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 20 - 100 °C

With 1,2,3-triazole; hydrogenchloride; N-ethyl-N,N-diisopropylamine; In 1,4-dioxane; diethyl ether; N,N-dimethyl-formamide; toluene;