2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

Base Information

Chemical Name:2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate
CAS No.:111471-82-0
Molecular Formula:C₁₉H₂₄O₆S₂
Molecular Weight:412.528
Hs Code.:

Synonyms:2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

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Chemical Property of 2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

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Technology Process of 2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

There total 3 articles about 2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 101746-78-5
2-(2-Methylbenzhydryl)propane-1,3-diol

: 124-63-0
methanesulfonyl chloride

: 111471-82-0
2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

Guidance literature:: With pyridine;
DOI:10.1071/CH9951707

Reference yield:

: 172876-85-6
Diethyl (2-Methylbenzhydryl)malonate

: 111471-82-0
2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / LiAlH₄ / diethyl ether / Heating

2: 99 percent / pyridine

With pyridine; lithium aluminium tetrahydride; In diethyl ether;
DOI:10.1071/CH9951707

Reference yield:

: 5292-53-5
diethyl benzalmalonate

: 111471-82-0
2-(2-Methylbenzhydryl)propane-1,3-diol bismethanesulfonate

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Mg / 1.) THF, reflux, benzene, reflux

2: 97 percent / LiAlH₄ / diethyl ether / Heating

3: 99 percent / pyridine

With pyridine; lithium aluminium tetrahydride; magnesium; In diethyl ether;
DOI:10.1071/CH9951707