phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

Base Information

Chemical Name:phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate
CAS No.:1075736-82-1
Molecular Formula:C₂₀H₁₇N₅O₂
Molecular Weight:359.387
Hs Code.:

Synonyms:phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

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Chemical Property of phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

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Technology Process of phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

There total 3 articles about phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 437604-16-5
3-iodobenzoic acid benzyl ester

: 5326-80-7
6-methyl-1H-pyrazolo[3,4-d]pyrimidin-4-amine

: 1075736-82-1
phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

Guidance literature:: With potassium carbonate; copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; In N,N-dimethyl-formamide; at 110 ℃; for 17h;

Reference yield:

: 100-39-0
benzyl bromide

: 1075736-82-1
phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1.66 h / 20 - 24 °C

2: potassium carbonate / copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane / N,N-dimethyl-formamide / 17 h / 110 °C

With potassium carbonate; copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; In N,N-dimethyl-formamide;

Reference yield:

: 618-51-9
3-Iodobenzoic acid

: 1075736-82-1
phenylmethyl 3-(4-amino-6-methyl-1H-pyrazolo[3,4-d]pyrimidin-1-yl)benzoate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / N,N-dimethyl-formamide / 1.66 h / 20 - 24 °C

2: potassium carbonate / copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane / N,N-dimethyl-formamide / 17 h / 110 °C

With potassium carbonate; copper(l) iodide; (R,R)-N,N'-dimethyl-1,2-diaminocyclohexane; In N,N-dimethyl-formamide;