C₅₆H₅₇Br₅N₄O₉Si

Base Information

Chemical Name:C₅₆H₅₇Br₅N₄O₉Si
CAS No.:250282-07-6
Molecular Formula:C₅₆H₅₇Br₅N₄O₉Si
Molecular Weight:1357.7
Hs Code.:

C<sub>56</sub>H<sub>57</sub>Br<sub>5</sub>N<sub>4</sub>O<sub>9</sub>Si

Synonyms:C₅₆H₅₇Br₅N₄O₉Si

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Chemical Property of C₅₆H₅₇Br₅N₄O₉Si

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Technology Process of C₅₆H₅₇Br₅N₄O₉Si

There total 16 articles about C₅₆H₅₇Br₅N₄O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36438-64-9
p-benzyloxystyrene

: 250282-07-6
C₅₆H₅₇Br₅N₄O₉Si

Guidance literature:: Multi-step reaction with 16 steps

1.1: 96 percent / Sharpless AD-mix-α

2.1: 93 percent / pyridine / CH₂Cl₂ / 0 °C

3.1: 87 percent / NaN₃ / CH₂Cl₂ / 50 °C

4.1: 97 percent / imidazole / dimethylformamide / 20 °C

5.1: 95 percent / PPh₃; H₂O / tetrahydrofuran / 20 °C

6.1: 98 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 20 °C

7.1: 82 percent / NBS / dimethylformamide / 20 °C

8.1: 68 percent / NaH / dimethylformamide / 90 °C

9.1: 95 percent / NaBH₄ / tetrahydrofuran; methanol / 20 °C

10.1: 92 percent / PPh₃; I₂; imidazole / tetrahydrofuran / 20 °C

11.1: 98 percent / dimethylformamide / 40 °C

12.1: NaBH₄; CoCl₂ / methanol / 0 °C

13.1: 67 percent / tetrahydrofuran

14.1: 78 percent / NBS / acetonitrile / 80 °C

15.1: 95 percent / LiOH (3N) / methanol; tetrahydrofuran / 20 °C

16.1: CF₃COOH / tetrahydrofuran / 20 °C

16.2: EDC; HOBt / dimethylformamide

With pyridine; 1H-imidazole; lithium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; sodium azide; Sharpless AD-mix-α; water; hydrogen; iodine; sodium hydride; triphenylphosphine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: Addition / 2.1: Tosylation / 3.1: azidation / 4.1: silylation / 5.1: Acetylation / 6.1: Hydrogenolysis / 7.1: Bromination / 8.1: Arylation / 9.1: Reduction / 10.1: Iodination / 11.1: Substitution / 12.1: Reduction / 13.1: Acylation / 14.1: Bromination / 15.1: Hydrolysis / 16.1: Elimination / 16.2: Cyclization;
DOI:10.1016/S0040-4039(99)01430-6

Reference yield:

: (S)-1-[4-(benzyloxy)phenyl]ethane-1,2-diol

: 250282-07-6
C₅₆H₅₇Br₅N₄O₉Si

Guidance literature:: Multi-step reaction with 15 steps

1.1: 93 percent / pyridine / CH₂Cl₂ / 0 °C

2.1: 87 percent / NaN₃ / CH₂Cl₂ / 50 °C

3.1: 97 percent / imidazole / dimethylformamide / 20 °C

4.1: 95 percent / PPh₃; H₂O / tetrahydrofuran / 20 °C

5.1: 98 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 20 °C

6.1: 82 percent / NBS / dimethylformamide / 20 °C

7.1: 68 percent / NaH / dimethylformamide / 90 °C

8.1: 95 percent / NaBH₄ / tetrahydrofuran; methanol / 20 °C

9.1: 92 percent / PPh₃; I₂; imidazole / tetrahydrofuran / 20 °C

10.1: 98 percent / dimethylformamide / 40 °C

11.1: NaBH₄; CoCl₂ / methanol / 0 °C

12.1: 67 percent / tetrahydrofuran

13.1: 78 percent / NBS / acetonitrile / 80 °C

14.1: 95 percent / LiOH (3N) / methanol; tetrahydrofuran / 20 °C

15.1: CF₃COOH / tetrahydrofuran / 20 °C

15.2: EDC; HOBt / dimethylformamide

With pyridine; 1H-imidazole; lithium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; sodium azide; water; hydrogen; iodine; sodium hydride; triphenylphosphine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: Tosylation / 2.1: azidation / 3.1: silylation / 4.1: Acetylation / 5.1: Hydrogenolysis / 6.1: Bromination / 7.1: Arylation / 8.1: Reduction / 9.1: Iodination / 10.1: Substitution / 11.1: Reduction / 12.1: Acylation / 13.1: Bromination / 14.1: Hydrolysis / 15.1: Elimination / 15.2: Cyclization;
DOI:10.1016/S0040-4039(99)01430-6

Reference yield:

: 250281-90-4
(S)-(+)-2-azido-1-(4-benzyloxyphenyl)-1-ethanol

: 250282-07-6
C₅₆H₅₇Br₅N₄O₉Si

Guidance literature:: Multi-step reaction with 13 steps

1.1: 97 percent / imidazole / dimethylformamide / 20 °C

2.1: 95 percent / PPh₃; H₂O / tetrahydrofuran / 20 °C

3.1: 98 percent / hydrogen / 10 percent Pd/C / ethyl acetate / 20 °C

4.1: 82 percent / NBS / dimethylformamide / 20 °C

5.1: 68 percent / NaH / dimethylformamide / 90 °C

6.1: 95 percent / NaBH₄ / tetrahydrofuran; methanol / 20 °C

7.1: 92 percent / PPh₃; I₂; imidazole / tetrahydrofuran / 20 °C

8.1: 98 percent / dimethylformamide / 40 °C

9.1: NaBH₄; CoCl₂ / methanol / 0 °C

10.1: 67 percent / tetrahydrofuran

11.1: 78 percent / NBS / acetonitrile / 80 °C

12.1: 95 percent / LiOH (3N) / methanol; tetrahydrofuran / 20 °C

13.1: CF₃COOH / tetrahydrofuran / 20 °C

13.2: EDC; HOBt / dimethylformamide

With 1H-imidazole; lithium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; water; hydrogen; iodine; sodium hydride; triphenylphosphine; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; methanol; ethyl acetate; N,N-dimethyl-formamide; acetonitrile; 1.1: silylation / 2.1: Acetylation / 3.1: Hydrogenolysis / 4.1: Bromination / 5.1: Arylation / 6.1: Reduction / 7.1: Iodination / 8.1: Substitution / 9.1: Reduction / 10.1: Acylation / 11.1: Bromination / 12.1: Hydrolysis / 13.1: Elimination / 13.2: Cyclization;
DOI:10.1016/S0040-4039(99)01430-6