3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Base Information

Chemical Name:3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure
CAS No.:173597-67-6
Molecular Formula:C₁₉H₂₀N₂O₈
Molecular Weight:404.376
Hs Code.:

Synonyms:3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Suppliers and Price of 3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

There total 3 articles about 3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 56-40-6,18875-39-3,25718-94-9
glycine

: 89080-61-5
1,3-Diacetyl-2-(3-nitrophenyl)propan-1,3-dicarbonsaeuredimethylester

: 173597-67-6
3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Guidance literature:: With pyridine; In methanol; for 144h; Heating;

Reference yield: 41.0%

: 99-61-6
3-nitro-benzaldehyde

: 105-45-3
acetoacetic acid methyl ester

: 56-40-6,18875-39-3,25718-94-9
glycine

: 173597-67-6
3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Guidance literature:: With pyridine; In methanol; for 504h; Heating;

Reference yield:

: 105-45-3
acetoacetic acid methyl ester

: 173597-67-6
3,5-Bis(methoxycarbonyl)-1,4-dihydro-2,6-dimethyl-4-(3-nitrophenyl)-1-pyridyl-essigsaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / ZnCl₂ / ethyl acetate / 1.) room temp., 15 min, 2.) 65 deg C, 6.5 h

2: 67 percent / pyridine / methanol / 144 h / Heating

With pyridine; zinc(II) chloride; In methanol; ethyl acetate;