1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

Base Information

Chemical Name:1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole
CAS No.:1430847-84-9
Molecular Formula:C₂₃H₂₆ClN₃O₄
Molecular Weight:443.93
Hs Code.:

Synonyms:1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

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Chemical Property of 1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

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Technology Process of 1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

There total 4 articles about 1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 14.5%

: 23010-10-8
t-butyl pyrocatechol

: 1360599-76-3
toluene-4-sulfonic acid 2-(4-chlorophenyl)-2-1H-[1,2,4]triazole-1-ylmethyl-[1,3]dioxolan-4-ylmethyl ester

: 1430847-84-9
1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 50 ℃;
DOI:10.1016/j.bmc.2013.03.006

Reference yield: 14.5%

: 1430847-84-9
1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

Guidance literature:: With potassium hydroxide; In N,N-dimethyl-formamide; at 50 ℃;

Reference yield:

: 536-38-9
4-chlorobenzoylmethyl bromide

: 1430847-84-9
1-[4-(2-tert-butoxyphenoxymethyl)-2-(4-chlorophenyl)-[1,3]-dioxolan-2-ylmethyl]-1H-[1,2,4]-triazole

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / acetone / 1.5 h / 0 - 20 °C

2: trifluorormethanesulfonic acid / 60 h / 20 °C / Inert atmosphere

3: potassium hydroxide / N,N-dimethyl-formamide / 50 °C

With trifluorormethanesulfonic acid; triethylamine; potassium hydroxide; In N,N-dimethyl-formamide; acetone;
DOI:10.1016/j.bmc.2013.03.006