ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

Base Information

Chemical Name:ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate
CAS No.:1254700-32-7
Molecular Formula:C₂₁H₁₇NO₄
Molecular Weight:347.37
Hs Code.:

Synonyms:ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

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Chemical Property of ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

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Technology Process of ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

There total 5 articles about ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 64.0%

: 2999-46-4
Ethyl isocyanoacetate

: 1261035-60-2
1-(2-iodophenyl)-3-(4-methoxyphenyl)prop-2-yn-1-one

: 1254700-32-7
ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

: C₂₁H₁₈INO₄

Guidance literature:: With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 90 ℃; for 0.166667h;
DOI:10.1021/ol102826f

Reference yield: 61.0%

: 2999-46-4
Ethyl isocyanoacetate

: 1258504-63-0
2-iodo-4'-methoxychalcone

: 1254700-32-7
ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

Guidance literature:: With copper(l) iodide; caesium carbonate; In N,N-dimethyl-formamide; at 20 ℃; In air;
DOI:10.1055/s-0030-1260171

Reference yield:

: C₁₆H₁₃IO₂

: 1254700-32-7
ethyl 3-(4-methoxyphenyl)-4-oxo-1,4-dihydroindeno[1,2-b]pyrrole-2-carboxylate

: C₂₁H₁₈INO₄

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane

2: copper(l) iodide; caesium carbonate / N,N-dimethyl-formamide / 0.17 h / 90 °C

With manganese(IV) oxide; copper(l) iodide; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ol102826f