(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

Base Information

Chemical Name:(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride
CAS No.:1449061-27-1
Molecular Formula:C₁₇H₁₆Cl₂N₂O₄*ClH
Molecular Weight:419.692
Hs Code.:

Synonyms:(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

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Chemical Property of (S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

Chemical Property:

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Technology Process of (S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

There total 5 articles about (S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449061-26-0
(S)-2-tert-butoxycarbonylamino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester

: 1449061-27-1
(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

Guidance literature:: With methanol; chloro-trimethyl-silane; at 20 ℃;

Reference yield:

: 216257-26-0
2,6-dichloro-4-triisopropylsilanyloxy-benzoic acid

: 1449061-27-1
(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: thionyl chloride / toluene / 2 h / Reflux

2: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

3: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

4: methanol; chloro-trimethyl-silane / 20 °C

With methanol; chloro-trimethyl-silane; thionyl chloride; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane; toluene;

Reference yield:

: 65615-90-9
(S)-methyl 3-(4-aminophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1449061-27-1
(S)-2-amino-3-[4-(2,6-dichloro-4-hydroxybenzoylamino)phenyl]propionic acid methyl ester hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3: methanol; chloro-trimethyl-silane / 20 °C

With methanol; chloro-trimethyl-silane; tetrabutyl ammonium fluoride; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; dichloromethane;