(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

Base Information

Chemical Name:(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid
CAS No.:1449061-37-3
Molecular Formula:C₆₀H₇₃Cl₃N₆O₁₉
Molecular Weight:1288.63
Hs Code.:

(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

Synonyms:(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

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Chemical Property of (S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

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Technology Process of (S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

There total 10 articles about (S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1449061-33-9
(S)-3-{4-[4-(3-aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

: 756525-93-6
3-[2-[2-[2-[2-[2-[2-[2-[[3-(2,5-dioxo-2,5-dihydro-pyrrol-1-yl)-propionylamino]-ethoxy]ethoxy]ethoxy]ethoxy]ethoxy]ethoxy] eth-5 oxy]ethoxy]-propionic acid-2,5-dioxo-pyrrolidin-1-yl ester

: 1449061-37-3
(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

Guidance literature:: With dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; at 20 ℃; for 1h;

Reference yield:

: 1449061-25-9
(S)-2-tert-butoxycarbonylamino-3-[4-(2,6-dichloro-4-triisopropylsilanyloxybenzoylamino)phenyl]propionic acid methyl ester

: 1449061-37-3
(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

Guidance literature:: Multi-step reaction with 7 steps

1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

2: methanol; chloro-trimethyl-silane / 20 °C

3: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

4: potassium carbonate / N,N-dimethyl-formamide; acetone / 75 °C

5: methanol; chloro-trimethyl-silane / 20 °C

6: water; sodium hydroxide / methanol / 20 °C

7: dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / 1 h / 20 °C

With methanol; chloro-trimethyl-silane; tetrabutyl ammonium fluoride; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; N,N-dimethyl-formamide; acetone;

Reference yield:

: 65615-90-9
(S)-methyl 3-(4-aminophenyl)-2-((tert-butoxycarbonyl)amino)propanoate

: 1449061-37-3
(S)-3-{4-[4-(3-(2-{2-[2-(2-{2-[2-(2-{2-ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)ethoxy]ethoxy}ethoxy)aminopropoxy)-2,6-dichlorobenzoylamino]phenyl}-2-[2-chloro-4-(3-hydroxybenzylcarbamoyl)benzoylamino]propionic acid

Guidance literature:: Multi-step reaction with 8 steps

1: N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C

2: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3: methanol; chloro-trimethyl-silane / 20 °C

4: N-ethyl-N,N-diisopropylamine; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / N,N-dimethyl-formamide / 20 °C

5: potassium carbonate / N,N-dimethyl-formamide; acetone / 75 °C

6: methanol; chloro-trimethyl-silane / 20 °C

7: water; sodium hydroxide / methanol / 20 °C

8: dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / 1 h / 20 °C

With methanol; chloro-trimethyl-silane; tetrabutyl ammonium fluoride; water; potassium carbonate; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; sodium hydroxide; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide; acetone;