C₃₃H₃₈BrNO₃

Base Information

Chemical Name:C₃₃H₃₈BrNO₃
CAS No.:1463522-96-4
Molecular Formula:C₃₃H₃₈BrNO₃
Molecular Weight:576.574
Hs Code.:

C<sub>33</sub>H<sub>38</sub>BrNO<sub>3</sub>

Synonyms:C₃₃H₃₈BrNO₃

Suppliers and Price of C₃₃H₃₈BrNO₃

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of C₃₃H₃₈BrNO₃

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of C₃₃H₃₈BrNO₃

There total 8 articles about C₃₃H₃₈BrNO₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 20769-85-1
2-bromoisobutyric acid bromide

: 1463523-08-1
C₂₉H₃₃NO₂

: 1463522-96-4
C₃₃H₃₈BrNO₃

Guidance literature:: With dmap; triethylamine; In dichloromethane; at -10 - 20 ℃;
DOI:10.1039/c3cc44799e

Reference yield:

: 99-05-8,159139-79-4
meta-aminobenzoic acid

: 1463522-96-4
C₃₃H₃₈BrNO₃

Guidance literature:: Multi-step reaction with 8 steps

1: sulfuric acid / Reflux

2: triethylamine / dichloromethane / 20 °C

3: tetrahydrofuran / 20 °C / Cooling with ice

4: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 3 h / Reflux

5: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

6: dioxomolybdenum(VI) dichloride; triethylamine / toluene / 3 h / 120 °C

7: toluene / 5 h / 120 °C

8: dmap; triethylamine / dichloromethane / -10 - 20 °C

With dmap; lithium aluminium tetrahydride; sulfuric acid; tetra-(n-butyl)ammonium iodide; dioxomolybdenum(VI) dichloride; sodium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene;
DOI:10.1039/c3cc44799e

Reference yield:

: 52189-36-3
methyl 5-acetylaminobenzoate

: 1463522-96-4
C₃₃H₃₈BrNO₃

Guidance literature:: Multi-step reaction with 6 steps

1: tetrahydrofuran / 20 °C / Cooling with ice

2: lithium aluminium tetrahydride / tetrahydrofuran; diethyl ether / 3 h / Reflux

3: sodium carbonate; tetra-(n-butyl)ammonium iodide / acetone; toluene / 2.5 h / Reflux

4: dioxomolybdenum(VI) dichloride; triethylamine / toluene / 3 h / 120 °C

5: toluene / 5 h / 120 °C

6: dmap; triethylamine / dichloromethane / -10 - 20 °C

With dmap; lithium aluminium tetrahydride; tetra-(n-butyl)ammonium iodide; dioxomolybdenum(VI) dichloride; sodium carbonate; triethylamine; In tetrahydrofuran; diethyl ether; dichloromethane; acetone; toluene;
DOI:10.1039/c3cc44799e