benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

Base Information

Chemical Name:benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate
CAS No.:1616347-64-8
Molecular Formula:C₂₀H₁₅F₆NO₃
Molecular Weight:431.334
Hs Code.:

Synonyms:benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

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Chemical Property of benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

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Technology Process of benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

There total 2 articles about benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 851726-81-3
benzyl {1-[methoxy(methyl)carbamoyl]cyclopropyl}carbamate

: 112981-69-8
3,5-bis(trifluoromethyl)phenylmagnesium bromide

: 1616347-64-8
benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

Guidance literature:: benzyl {1-[methoxy(methyl)carbamoyl]cyclopropyl}carbamate; With TurboGrignard; In tetrahydrofuran; at -15 ℃; for 0.25h; Inert atmosphere;

3,5-bis(trifluoromethyl)phenylmagnesium bromide; With TurboGrignard; In tetrahydrofuran; at 20 ℃;

Reference yield:

: 84677-06-5
(benzyloxycarbonylamino)cyclopropanecarboxylic acid

: 1616347-64-8
benzyl (1-{[3,5-bis(trifluoromethyl)phenyl]carbonyl}cyclopropyl)carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: triethylamine; HATU / N,N-dimethyl-formamide / 3 h / 20 °C / Inert atmosphere

2.1: TurboGrignard / tetrahydrofuran / 0.25 h / -15 °C / Inert atmosphere

2.2: 20 °C

With TurboGrignard; triethylamine; HATU; In tetrahydrofuran; N,N-dimethyl-formamide;