Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

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Chemical Name:Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine
CAS No.:866925-84-0
Molecular Formula:C₃₆H₄₃NO₃Si
Molecular Weight:565.828
Hs Code.:

Synonyms:Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

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Chemical Property of Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

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Technology Process of Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

There total 3 articles about Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 857294-02-1
(1R)-N-benzyl-N-[2-(tert-butyldiphenylsilyloxy)-1-(2,2-dimethyl-[1,3]dioxolan-4(R)-yl)-1-phenylethyl]hydroxylamine

: 866925-84-0
Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

Guidance literature:: With copper; acetic acid; zinc; for 0.583333h; Heating;
DOI:10.1016/j.tetasy.2005.03.013

Reference yield:

: 100-59-4
phenylmagnesium chloride

: 866925-84-0
Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 5 h / -78 °C

2: 72 percent / Zn/Cu; acetic acid / 0.58 h / Heating

With copper; acetic acid; zinc; In tetrahydrofuran;
DOI:10.1016/j.tetasy.2005.03.013

Reference yield:

: 591-51-5
phenyllithium

: 866925-84-0
Benzyl-[(R)-2-(tert-butyl-diphenyl-silanyloxy)-1-((R)-2,2-dimethyl-[1,3]dioxolan-4-yl)-1-phenyl-ethyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1.1: diethyl aluminium chloride / diethyl ether / 0.25 h / cooling

1.2: diethyl ether / 5 h / -78 °C

2.1: 72 percent / Zn/Cu; acetic acid / 0.58 h / Heating

With diethylaluminium chloride; copper; acetic acid; zinc; In diethyl ether;
DOI:10.1016/j.tetasy.2005.03.013