Dithiocarbonic acid O-cyclohexyl S-potassium salt

Base Information

• Chemical Name: Dithiocarbonic acid O-cyclohexyl S-potassium salt
• CAS No.: 2720-77-6
• Molecular Formula: C7H12 O S2 . K
• Molecular Weight: 214.394
• Mol file: 2720-77-6.mol

Synonyms:Carbonicacid, dithio-, O-cyclohexyl ester, potassium salt (8CI); Carbonodithioic acid,O-cyclohexyl ester, potassium salt (9CI); Xanthic acid, cyclohexyl-, potassiumsalt (7CI); Cyclohexyl potassium xanthate; Potassium cyclohexyl xanthate;Potassium cyclohexyl xanthogenate

Chemical Property of Dithiocarbonic acid O-cyclohexyl S-potassium salt

Chemical Property:

• Vapor Pressure: 0.122mmHg at 25°C
• Boiling Point: 226.5°C at 760 mmHg
• Flash Point: 90.8°C
• PSA: 41.32000
• LogP: 2.16750

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Dithiocarbonic acid O-cyclohexyl S-potassium salt

There total 4 articles about Dithiocarbonic acid O-cyclohexyl S-potassium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

carbon disulfide (75-15-0,12122-00-8) + cyclohexanol (108-93-0) → potassium cyclohexyl xanthogenate (2720-77-6)

Guidance literature:

cyclohexanol; With potassium hydroxide; In tetrahydrofuran; for 1h; Reflux; Cooling with ice; Inert atmosphere;

carbon disulfide; In tetrahydrofuran; at 20 ℃; Cooling with ice; Inert atmosphere;

DOI:10.1002/hlca.201200311

Reference yield:

carbon disulfide (75-15-0,12122-00-8) → potassium cyclohexyl xanthogenate (2720-77-6)

Guidance literature:

With diethyl ether;

Reference yield:

carbon disulfide (75-15-0,12122-00-8) + diethyl ether (60-29-7,927820-24-4) → potassium cyclohexyl xanthogenate (2720-77-6)

Guidance literature:

With potassium hydroxide; cyclohexanol;

upstream raw materials:

carbon disulfide

diethyl ether

cyclohexanol

Downstream raw materials:

(6R)-3-cyclohexyloxythiocarbonylsulfanylmethyl-8-oxo-7t-(2-thiophen-2-yl-acetylamino)-(6rH)-5-thia-1-aza-bicyclo[4.2.0]oct-2-ene-2-carboxylic acid

((n)Bu)4N[Fe(cyclohexylxanthate)3]

Et₄N[Fe(cyclohexylxanthate)3]

trans-Fe(cyclohexylxanthate)2(3,5-dichloropyridine)2

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