3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

Base Information

Chemical Name:3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate
CAS No.:174811-13-3
Molecular Formula:C₃₉H₃₆N₂O₉S₂
Molecular Weight:740.855
Hs Code.:

Synonyms:3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

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Chemical Property of 3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

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Technology Process of 3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

There total 4 articles about 3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 148-18-5
sodium N,N-diethyldithiocarbamate

: 174811-12-2
3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-α-lyxo-hexopyranosyl bromide

: 174811-13-3
3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

Guidance literature:: With molecular sieve; In acetone; for 0.5h;
DOI:10.1248/cpb.44.15

Reference yield:

: 98-88-4
benzoyl chloride

: 174811-13-3
3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / 4 h

2: 90 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Heating; Irradiation

3: 84 percent / molecular sieves / acetone / 0.5 h

With pyridine; N-Bromosuccinimide; molecular sieve; In tetrachloromethane; acetone;
DOI:10.1248/cpb.44.15

Reference yield:

: 1,5-anhydro-3,4,6-tri-O-benzoyl-D-tagatose oxime

: 174811-13-3
3,4,6-tri-O-benzoyl-2-(benzoyloxyimino)-2-deoxy-β-lyxo-hexopyranosyl N,N-diethyldithiocarbonate

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / pyridine / 4 h

2: 90 percent / N-bromosuccinimide / CCl₄ / 0.5 h / Heating; Irradiation

3: 84 percent / molecular sieves / acetone / 0.5 h

With pyridine; N-Bromosuccinimide; molecular sieve; In tetrachloromethane; acetone;
DOI:10.1248/cpb.44.15