N,N-diphenylundec-10-enamide

Base Information

• Chemical Name: N,N-diphenylundec-10-enamide
• CAS No.: 52007-57-5
• Molecular Formula: C₂₃H₂₉NO
• Molecular Weight: 335.489
• Mol file: 52007-57-5.mol

Synonyms:N,N-diphenylundec-10-enamide

Chemical Property of N,N-diphenylundec-10-enamide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N,N-diphenylundec-10-enamide

There total 3 articles about N,N-diphenylundec-10-enamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

undec-10-enoyl chloride (38460-95-6) + diphenylamine (122-39-4) → N,N-diphenylundec-10-enamide (52007-57-5)

Guidance literature:

In toluene; for 3h; Reflux; Inert atmosphere;

DOI:10.1016/j.tet.2014.11.021

Reference yield: 60.0%

10-undecenoic acid (112-38-9) + diphenylamine (122-39-4) → N,N-diphenylundec-10-enamide (52007-57-5)

Guidance literature:

With triethylamine; trichlorophosphate; In dichloromethane;

Reference yield:

12-chloro-13,13,13-trifluoro-N,N-diphenyltridecanamide → N,N-diphenylundec-10-enamide (52007-57-5)

Guidance literature:

Multi-step reaction with 2 steps

1: magnesium; ethylene dibromide / tetrahydrofuran / Reflux; Inert atmosphere

2: toluene / 3 h / Reflux; Inert atmosphere

With magnesium; ethylene dibromide; In tetrahydrofuran; toluene;

DOI:10.1016/j.tet.2014.11.021

upstream raw materials:

10-undecenoic acid

diphenylamine

undec-10-enoyl chloride

Downstream raw materials:

Diphenyl-undec-10-enyl-amine