2-(3-methoxyphenyl)-N-phenethylglutarimide

Base Information

Chemical Name:2-(3-methoxyphenyl)-N-phenethylglutarimide
CAS No.:79987-74-9
Molecular Formula:C₂₀H₂₁NO₃
Molecular Weight:323.392
Hs Code.:

Synonyms:2-(3-methoxyphenyl)-N-phenethylglutarimide

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Chemical Property of 2-(3-methoxyphenyl)-N-phenethylglutarimide

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Technology Process of 2-(3-methoxyphenyl)-N-phenethylglutarimide

There total 5 articles about 2-(3-methoxyphenyl)-N-phenethylglutarimide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 19924-43-7
3-methoxyphenylacetonitrile

: 79987-74-9
2-(3-methoxyphenyl)-N-phenethylglutarimide

Guidance literature:: Multi-step reaction with 5 steps

1: lithium diisopropylamide / tetrahydrofuran

2: 25percent sulfuric acid, 8N chromic acid / acetone

3: KOH / ethanol; H₂O / 6 h / Heating

4: 74 percent / acetic anhydride / 3 h / Heating

5: 2.) acetic anhydride / 1.) benzene, 1 h, reflux; 2.) 5 h, reflux

With potassium hydroxide; sulfuric acid; acetic anhydride; chromic acid; lithium diisopropyl amide; In tetrahydrofuran; ethanol; water; acetone;
DOI:10.1002/recl.19811000909

Reference yield:

: 79987-85-2
4-cyano-4-(3-methoxyphenyl)butyric acid

: 79987-74-9
2-(3-methoxyphenyl)-N-phenethylglutarimide

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol; H₂O / 6 h / Heating

2: 74 percent / acetic anhydride / 3 h / Heating

3: 2.) acetic anhydride / 1.) benzene, 1 h, reflux; 2.) 5 h, reflux

With potassium hydroxide; acetic anhydride; In ethanol; water;
DOI:10.1002/recl.19811000909

Reference yield:

: 79987-86-3
2-(3-Methoxy-phenyl)-5-(tetrahydro-pyran-2-yloxy)-pentanenitrile

: 79987-74-9
2-(3-methoxyphenyl)-N-phenethylglutarimide

Guidance literature:: Multi-step reaction with 4 steps

1: 25percent sulfuric acid, 8N chromic acid / acetone

2: KOH / ethanol; H₂O / 6 h / Heating

3: 74 percent / acetic anhydride / 3 h / Heating

4: 2.) acetic anhydride / 1.) benzene, 1 h, reflux; 2.) 5 h, reflux

With potassium hydroxide; sulfuric acid; acetic anhydride; chromic acid; In ethanol; water; acetone;
DOI:10.1002/recl.19811000909