dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

Base Information

Chemical Name:dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate
CAS No.:1229521-08-7
Molecular Formula:C₃₅H₃₇N₂O₇P
Molecular Weight:628.662
Hs Code.:

Synonyms:dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

Chemical Property:

Purity/Quality:

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MSDS Files:: SDS file from LookChem

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Technology Process of dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

There total 2 articles about dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 61.1%

: 1623-08-1
phosphoric acid dibenzyl ester

: 1229521-07-6
4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

: 1229521-08-7
dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

Guidance literature:: With N-iodo-succinimide; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/jps.22021

Reference yield:

: 23111-33-3
4-n-Butyl-4-hydroxymethyl-1,2-diphenyl-3,5-dioxopyrazolidin

: 1229521-08-7
dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

Guidance literature:: Multi-step reaction with 2 steps

1: acetic anhydride; acetic acid / 24 h / 20 °C / Inert atmosphere

2: N-iodo-succinimide / tetrahydrofuran / 12 h / 20 °C

With N-iodo-succinimide; acetic anhydride; acetic acid; In tetrahydrofuran;
DOI:10.1002/jps.22021

Reference yield:

: 1229521-08-7
dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

: 50-33-9,4297-92-1
Phenylbutazone

Guidance literature:: Multi-step reaction with 3 steps

1: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C

2: sodium hydroxide / ethanol; water

3: human placental alkaline phosphatase; magnesium chloride; zinc(II) chloride / 37 °C / pH 7.4 / aq. buffer; Enzymatic reaction

With human placental alkaline phosphatase; palladium 10% on activated carbon; hydrogen; sodium hydroxide; magnesium chloride; zinc(II) chloride; In ethanol; water;
DOI:10.1002/jps.22021