4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

Base Information

Chemical Name:4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione
CAS No.:1229521-07-6
Molecular Formula:C₂₂H₂₆N₂O₃S
Molecular Weight:398.526
Hs Code.:

Synonyms:4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

Chemical Property:

Purity/Quality:

Safty Information:

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Hazard Codes:

MSDS Files:: SDS file from LookChem

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Technology Process of 4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

There total 1 articles about 4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.7%

: 23111-33-3
4-n-Butyl-4-hydroxymethyl-1,2-diphenyl-3,5-dioxopyrazolidin

: 67-68-5,8070-53-9
dimethyl sulfoxide

: 1229521-07-6
4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

Guidance literature:: With acetic anhydride; acetic acid; at 20 ℃; for 24h; Inert atmosphere;
DOI:10.1002/jps.22021

Reference yield: 61.1%

: 1623-08-1
phosphoric acid dibenzyl ester

: 1229521-07-6
4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

: 1229521-08-7
dibenzyl ((4-butyl-3,5-dioxo-1,2-diphenylpyrazolidin-4-yl)methoxy)methyl phosphate

Guidance literature:: With N-iodo-succinimide; In tetrahydrofuran; at 20 ℃; for 12h;
DOI:10.1002/jps.22021

Reference yield:

: 1229521-07-6
4-butyl-4-((methylthiomethoxy)methyl)-1,2-diphenylpyrazolidine-3,5-dione

: 50-33-9,4297-92-1
Phenylbutazone

Guidance literature:: Multi-step reaction with 4 steps

1: N-iodo-succinimide / tetrahydrofuran / 12 h / 20 °C

2: palladium 10% on activated carbon; hydrogen / ethanol / 6 h / 20 °C

3: sodium hydroxide / ethanol; water

4: human placental alkaline phosphatase; magnesium chloride; zinc(II) chloride / 37 °C / pH 7.4 / aq. buffer; Enzymatic reaction

With N-iodo-succinimide; human placental alkaline phosphatase; palladium 10% on activated carbon; hydrogen; sodium hydroxide; magnesium chloride; zinc(II) chloride; In tetrahydrofuran; ethanol; water;
DOI:10.1002/jps.22021