(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

Base Information

Chemical Name:(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium
CAS No.:105501-02-8
Molecular Formula:C₂₆H₃₄Zr
Molecular Weight:437.78
Hs Code.:

Synonyms:(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

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Technology Process of (pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

There total 4 articles about (pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 79847-76-0
diphenylpermethylzirconocene

: 105501-02-8
(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

Guidance literature:: In toluene; soln. of the complex in toluene was heated at 100°C for 6 h;; toluene was evapd., pentane was condensed into the reaction vessel; soln. was stirred, warmed to dissolve all product and slowly cooled to -78°C, crystals were collected and dried in vac.; elem. anal.;;

Reference yield: 90.0%

: 112532-20-4
Cp'2Zr(H)Ph

: 105501-02-8
(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

Guidance literature:: In benzene; byproducts: H2; Soln. is degassed and thermolyzed at 150°C for 4 h, mixt. is quickly cooled to -196°C and H2 is pumped off, this procedure is repeated 4-5 times.; Solvent is vac. distd. from the sample, orange oil is washed (petroleum ether), evapn., recrystn. (-78°C, petroleum ether);

Reference yield:

: 61396-34-7
(pentamethylcyclopentadienyl)2ZrH₂

: 105501-02-8
(pentamethylcyclopentadienyl)(π-η(5):σ-η(1)-tetramethylfulvene)phenylzirconium

Guidance literature:: In benzene; byproducts: H2; Soln. is degassed and thermolyzed at 150°C for 4 h, mixt. is quickly cooled to -196°C and H2 is pumped off, this procedure is repeated 6-7 times.; Evapn., recrystn. (-78°C, petroleum ether);