3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

Base Information

Chemical Name:3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt
CAS No.:726190-93-8
Molecular Formula:C₁₀H₁₁N₃O₃
Molecular Weight:221.216
Hs Code.:

Synonyms:3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

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Chemical Property of 3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

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Technology Process of 3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

There total 1 articles about 3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 240431-48-5
3-hydroxy-5-[[imino-(methylthio)-methyl]amino]benzoic acid monohydroiodide

: 107-15-3,85404-18-8
ethylenediamine

: 726190-93-8
3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

Guidance literature:: In DMF (N,N-dimethyl-formamide); at 75 ℃;

Reference yield: 31.0%

: ethyl (3R)-3-(N-Gly)amino-3-(3-bromo-5-chloro-2-hydroxyphenyl)propanoate hydrochloride

: 726190-93-8
3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

: C₂₃H₂₅BrClN₅O₆

Guidance literature:: 3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt; With trifluoroacetic acid; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.166667h;

With benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; In DMF (N,N-dimethyl-formamide); at 20 ℃; for 0.5h;

ethyl (3R)-3-(N-Gly)amino-3-(3-bromo-5-chloro-2-hydroxyphenyl)propanoate hydrochloride; With triethylamine; In DMF (N,N-dimethyl-formamide); for 18h;

Reference yield:

: 726190-93-8
3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt

: 1541197-63-0
(S)-3-(2-aminoacetylamino)-3-(3-bromo-5-tert-butylphenyl)propionic acid ethyl ester hydrochloride salt

: 1541198-89-3
(S)-ethyl 3-(3-bromo-5-(tert-butyl)phenyl)-3-(2-(3-((4,5-dihydro-1H-imidazol-2-yl)amino)-5-hydroxybenzamido)acetamido)propanoate

Guidance literature:: 3[(4,5-dihydro-1H-imidazol-2y)amino]-5-hydroxy benzoic acid formic acid salt; (S)-3-(2-aminoacetylamino)-3-(3-bromo-5-tert-butylphenyl)propionic acid ethyl ester hydrochloride salt; With benzotriazol-1-ol; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; for 0.166667h; Inert atmosphere;

With diisopropyl-carbodiimide; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;