3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

Base Information

Chemical Name:3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile
CAS No.:1359741-26-6
Molecular Formula:C₆₂H₉₃NO₆
Molecular Weight:948.424
Hs Code.:

Synonyms:3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

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Chemical Property of 3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

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Technology Process of 3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

There total 6 articles about 3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 1359741-08-4
2-(4-(dodecyloxy)-3-methoxyphenyl)acetonitrile

: 1359741-25-5
3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthrene-9-carbaldehyde

: 1359741-26-6
3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

Guidance literature:: With sodium ethanolate; In ethanol; for 3h; Reflux;
DOI:10.1021/ja210991f

Reference yield:

: 112-29-8
1-bromo dodecane

: 1359741-26-6
3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 65 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 2 h / Reflux

3.1: iron(III) chloride; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / Inert atmosphere

4.2: Inert atmosphere

5.1: sodium ethanolate / ethanol / 3 h / Reflux

With iron(III) chloride; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja210991f

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1359741-26-6
3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-2-(4-(dodecyloxy)-3-methoxyphenyl)acrylonitrile

Guidance literature:: Multi-step reaction with 5 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 65 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 2 h / Reflux

3.1: iron(III) chloride; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / Inert atmosphere

4.2: Inert atmosphere

5.1: sodium ethanolate / ethanol / 3 h / Reflux

With iron(III) chloride; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja210991f