(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

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Chemical Name:(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol
CAS No.:1359741-28-8
Molecular Formula:C₆₄H₉₇NO₇
Molecular Weight:992.477
Hs Code.:

Synonyms:(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

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Chemical Property of (3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

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Technology Process of (3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

There total 9 articles about (3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1359741-27-7
ethyl 3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrole-2-carboxylate

: 1359741-28-8
(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

Guidance literature:: With lithium aluminium tetrahydride; In tetrahydrofuran; for 1h; Inert atmosphere;
DOI:10.1021/ja210991f

Reference yield:

: 112-29-8
1-bromo dodecane

: 1359741-28-8
(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 65 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 2 h / Reflux

3.1: iron(III) chloride; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / Inert atmosphere

4.2: Inert atmosphere

5.1: sodium ethanolate / ethanol / 3 h / Reflux

6.1: potassium tert-butylate / tetrahydrofuran / 168 h / 0 °C / Inert atmosphere

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Inert atmosphere

With iron(III) chloride; lithium aluminium tetrahydride; potassium tert-butylate; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja210991f

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 1359741-28-8
(3-(3,6-bis(dodecyloxy)-2,7-dimethoxyphenanthren-9-yl)-4-(4-(dodecyloxy)-3-methoxyphenyl)-1H-pyrrol-2-yl)methanol

Guidance literature:: Multi-step reaction with 7 steps

1.1: potassium carbonate / N,N-dimethyl-formamide / 48 h / 65 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 2 h / Reflux

3.1: iron(III) chloride; 3-chloro-benzenecarboperoxoic acid / dichloromethane / 1 h / Inert atmosphere

4.1: diisobutylaluminium hydride / hexane; dichloromethane / Inert atmosphere

4.2: Inert atmosphere

5.1: sodium ethanolate / ethanol / 3 h / Reflux

6.1: potassium tert-butylate / tetrahydrofuran / 168 h / 0 °C / Inert atmosphere

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 1 h / Inert atmosphere

With iron(III) chloride; lithium aluminium tetrahydride; potassium tert-butylate; sodium ethanolate; diisobutylaluminium hydride; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In tetrahydrofuran; ethanol; hexane; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja210991f